SIST EN 16852:2017

Foodstuffs - Determination of ethyl carbamate in stone fruit spirits, fruit marc spirits and other spirit drinks - GC-MS method

This European Standard specifies a gas chromatographic method using mass spectrometric detection for the determination of ethyl carbamate (EC) in stone fruit spirits, fruit marc spirits and other spirit drinks.
The method has been validated in an interlaboratory study for stone fruit spirits and fruit liqueurs, at levels ranging from 0,253 mg/l to 1,11 mg/l. However, linearity of the instrument response was proven for the concentration range 0,10 mg/l to 4,0 mg/l (simplified method) and 0,025 mg/l to 3,0 mg/l (procedure including sample clean-up), respectively.

Lebensmittel - Bestimmung von Ethylcarbamat in Steinobstbränden, Obstbränden und anderen alkoholischen Getränken - GC-MS-Verfahren

Dieses Dokument legt ein Verfahren zur Bestimmung von Ethylcarbamat (EC) in Steinobstbränden, Obst¬bränden und anderen alkoholischen Getränken mit Gaschromatographie und Massenspektrometrie (GC-MS) fest.
Das Verfahren wurde in einem Ringversuch für Steinobstbrände und Obstliköre im Bereich von 0,253 mg/l bis 1,11 mg/l validiert. Die Linearität des Ansprechverhaltens des Gerätes wurde jedoch für den Konzentrations-bereich von 0,10 mg/l bis 4,0 mg/l (vereinfachtes Verfahren) und von 0,025 mg/l bis 3,0 mg/l (Verfahren mit Probenreinigung) nachgewiesen.

Produits alimentaires - Détermination de la teneur en carbamate d'éthyle dans les eaux-de-vie de fruits à noyaux, les eaux-de-vie de marc de fruits et les autres boissons alcoolisées - Méthode CG-SM

Le présent document spécifie une méthode de détermination de la teneur en carbamate d’éthyle (CE) par chromatographie en phase gazeuse couplée à une détection spectrométrique de masse dans les eaux-de-vie de fruits à noyaux, les eaux-de-vie de marc de fruits et les autres boissons spiritueuses.
La méthode a été validée lors d’un essai interlaboratoires sur les eaux-de-vie de fruits à noyaux et les liqueurs de fruits, à des niveaux compris entre 0,253 mg/l et 1,11 mg/l. Toutefois, la linéarité de la réponse de l’instrument a été prouvée pour la gamme de concentration de 0,10 mg/l à 4,0 mg/l (méthode simplifiée) et de 0,025 mg/l à 3,0 mg/l (mode opératoire comprenant la purification de l’échantillon), respectivement.

Živila - Ugotavljanje etil karbamata v žganju iz koščičastega sadja, sadnih tropin in drugih žganih pijačah - Metoda GC-MS

Ta evropski standard določa metodo plinske kromatografije z uporabo masne spektrometrične detekcije za ugotavljanje etil karbamata v žganju iz koščičastega sadja, sadnih tropin in drugih žganih pijačah.
Ta metoda je bila validirana v medlaboratorijski študiji o žganju iz koščičastega sadja in sadnih likerjih v obsegu 0,253–1,11 mg/l. Kljub temu je bil linearni odziv instrumenta dokazan za koncentracije 0,10–4,0 mg/l (poenostavljena metoda) in 0,025–3,0 mg/l (postopek, vključno s čiščenjem vzorcev).

General Information

• Status: Published
• Public Enquiry End Date: 29-Jul-2015
• Publication Date: 05-Jun-2017
• ICS: 67.160.10 - Alcoholic beverages
• Technical Committee: KŽP - Agricultural food products
• Current Stage: 6060 - National Implementation/Publication (Adopted Project)
• Start Date: 05-May-2017
• Due Date: 10-Jul-2017
• Completion Date: 06-Jun-2017
• Directive: 2014/34/EU - Directive 2014/34/EU Of The European Parliament And Of The Council of 26 February 2014 on the harmonisation of the laws of the Member States relating to equipment and protective systems intended for use in potentially explosive atmospheres (recast)
• Directive: 882/2004 - Regulation (EC) No 882/2004 of the European Parliament and of the Council of 29 April 2004 onofficial controls performed to ensure the verification of compliance with feed and food law, animal health and animal welfare rules
• Mandate: M/463 - Mandate for Standardisation addressed to CEN for the methods of analysis for food contaminants
• Ref Project: EN 16852:2017 - Foodstuffs - Determination of ethyl carbamate in stone fruit spirits, fruit marc spirits and other spirit drinks - GC-MS method

Standards Content (Sample)

2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.Lebensmittel - Bestimmung von Ethylcarbamat in Steinobstbränden, Obstbränden und anderen alkoholischen Getränken - GC-MS-VerfahrenProduits alimentaires - Détermination de la teneur en carbamate d'éthyle dans les eaux-de-vie de fruits à noyaux, les eaux-de-vie de marc de fruits et les autres boissons alcoolisées - Méthode CG-SMFoodstuffs - Determination of ethyl carbamate in stone fruit spirits, fruit marc spirits and other spirit drinks - GC-MS method67.160.10Alcoholic beveragesICS:Ta slovenski standard je istoveten z:EN 16852:2017SIST EN 16852:2017en,fr,de01-julij-2017SIST EN 16852:2017SLOVENSKI
STANDARD



SIST EN 16852:2017



EUROPEAN STANDARD NORME EUROPÉENNE EUROPÄISCHE NORM
EN 16852
May
t r s y ICS
x yä s x rä s r English Version
Foodstuffs æ Determination of ethyl carbamate in stone fruit spiritsá fruit marc spirits and other spirit drinks æ GCæMS method Produits alimentaires æ Détermination de la teneur en carbamate d 5éthyle dans les eauxædeævie de fruits à noyauxá les eauxædeævie de marc de fruits et les autres boissons alcoolisées æ Méthode par CGæSM
Lebensmittel æ Bestimmung von Ethylcarbamat in Steinobstbrändená Obstbränden und anderen Spirituosen æ GCæMSæVerfahren This European Standard was approved by CEN on
t r February
t r s yä
egulations which stipulate the conditions for giving this European Standard the status of a national standard without any alterationä Upætoædate lists and bibliographical references concerning such national standards may be obtained on application to the CENæCENELEC Management Centre or to any CEN memberä
translation under the responsibility of a CEN member into its own language and notified to the CENæCENELEC Management Centre has the same status as the official versionsä
CEN members are the national standards bodies of Austriaá Belgiumá Bulgariaá Croatiaá Cyprusá Czech Republicá Denmarká Estoniaá Finlandá Former Yugoslav Republic of Macedoniaá Franceá Germanyá Greeceá Hungaryá Icelandá Irelandá Italyá Latviaá Lithuaniaá Luxembourgá Maltaá Netherlandsá Norwayá Polandá Portugalá Romaniaá Serbiaá Slovakiaá Sloveniaá Spainá Swedená Switzerlandá Turkey and United Kingdomä
EUROPEAN COMMITTEE FOR STANDARDIZATION COMITÉ EUROPÉEN DE NORMALISATION EUROPÄISCHES KOMITEE FÜR NORMUNG
CEN-CENELEC Management Centre:
Avenue Marnix 17,
B-1000 Brussels
9
t r s y CEN All rights of exploitation in any form and by any means reserved worldwide for CEN national Membersä Refä Noä EN
s x z w tã t r s y ESIST EN 16852:2017



EN 16852:2017 (E) 2 Contents Page European foreword . 3 1 Scope . 4 2 Normative references . 4 3 Principle . 4 4 Reagents . 4 5 Apparatus . 7 6 Procedure. 8 7 Gas chromatography and mass spectrometry (GC-MS) . 9 8 Calculation . 9 9 Precision . 10 10 Test report . 11 Annex A (informative)
Typical chromatograms . 12 Annex B (informative)
Precision data . 16 Bibliography . 17
SIST EN 16852:2017



EN 16852:2017 (E) 3 European foreword This document (EN 16852
...