Test methods for repair materials for water-leakage cracks in underground concrete structures — Part 2: Test method for chemical resistance

ISO/TS 17774-2:2016 specifies a laboratory test method for the qualitative determination of the retention level of chemical resistance of repair materials in repaired cracks of concrete structures in conditions where the material is either underwater or in contact with water that may have various chemical components present.

Méthodes d'essai pour matériaux de réparation pour fissures dues à l'eau dans les structures en béton souterraines — Partie 2: Méthode d'essai de la résistance chimique

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Status
Withdrawn
Publication Date
21-Jul-2016
Current Stage
9599 - Withdrawal of International Standard
Completion Date
24-Apr-2023
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ISO/TS 16774-2:2016 - Test methods for repair materials for water-leakage cracks in underground concrete structures
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TECHNICAL ISO/TS
SPECIFICATION 16774-2
First edition
2016-08-01
Test methods for repair materials for
water-leakage cracks in underground
concrete structures —
Part 2:
Test method for chemical resistance
Méthodes d’essai pour matériaux de réparation pour fissures dues à
l’eau dans les structures en béton souterraines —
Partie 2: Méthode d’essai de la résistance chimique
Reference number
ISO/TS 16774-2:2016(E)
©
ISO 2016

---------------------- Page: 1 ----------------------
ISO/TS 16774-2:2016(E)

COPYRIGHT PROTECTED DOCUMENT
© ISO 2016, Published in Switzerland
All rights reserved. Unless otherwise specified, no part of this publication may be reproduced or utilized otherwise in any form
or by any means, electronic or mechanical, including photocopying, or posting on the internet or an intranet, without prior
written permission. Permission can be requested from either ISO at the address below or ISO’s member body in the country of
the requester.
ISO copyright office
Ch. de Blandonnet 8 • CP 401
CH-1214 Vernier, Geneva, Switzerland
Tel. +41 22 749 01 11
Fax +41 22 749 09 47
copyright@iso.org
www.iso.org
ii © ISO 2016 – All rights reserved

---------------------- Page: 2 ----------------------
ISO/TS 16774-2:2016(E)

Contents Page
Foreword .iv
Introduction .v
1 Scope . 1
2 Normative references . 1
3 Terms and definitions . 1
4 Principle . 1
5 Apparatus . 2
6 Preparation . 2
6.1 Test specimens . 2
6.2 Chemical substance . 2
6.3 Ambient conditions . 2
7 Procedure. 3
8 Expression of results . 3
9 Test report . 3
9.1 Information on the repair material of the test target . 3
9.1.1 General. 3
9.1.2 Other information . 4
9.2 Information on the test . 4
Annex A (informative) Example test method . 5
Bibliography . 8
© ISO 2016 – All rights reserved iii

---------------------- Page: 3 ----------------------
ISO/TS 16774-2:2016(E)

Foreword
ISO (the International Organization for Standardization) is a worldwide federation of national standards
bodies (ISO member bodies). The work of preparing International Standards is normally carried out
through ISO technical committees. Each member body interested in a subject for which a technical
committee has been established has the right to be represented on that committee. International
organizations, governmental and non-governmental, in liaison with ISO, also take part in the work.
ISO collaborates closely with the International Electrotechnical Commission (IEC) on all matters of
electrotechnical standardization.
The procedures used to develop this document and those intended for its further maintenance are
described in the ISO/IEC Directives, Part 1. In particular the different approval criteria needed for the
different types of ISO documents should be noted. This document was drafted in accordance with the
editorial rules of the ISO/IEC Directives, Part 2 (see www.iso.org/directives).
Attention is drawn to the possibility that some of the elements of this document may be the subject of
patent rights. ISO shall not be held responsible for identifying any or all such patent rights. Details of
any patent rights identified during the development of the document will be in the Introduction and/or
on the ISO list of patent declarations received (see www.iso.org/patents).
Any trade name used in this document is information given for the convenience of users and does not
constitute an endorsement.
For an explanation on the meaning of ISO specific terms and expressions related to conformity assessment,
as well as information about ISO’s adherence to the World Trade Organization (WTO) principles in the
Technical Barriers to Trade (TBT) see the following URL: www.iso.org/iso/foreword.html.
The committee responsible for this document is ISO/TC 71, Concrete, reinforced concrete and pre-
stressed concrete, Subcommittee SC 7, Maintenance and repair of concrete structures.
ISO/TS 16774 consist of the following parts, under the general title Test methods for repair materials for
water-leakage cracks in underground concrete structures:
— Part 2: Test method for chemical resistance
— Part 3: Test method for water (wash out) resistance
— Part 4: Test method for adhesion on wet concrete surface
The following parts are under preparation:
— Part 1: Test method for thermal stability
— Part 5: Test method for watertightness
— Part 6: Test method for response to the substrate movement
iv © ISO 2016 – All rights reserved

---------------------- Page: 4 ----------------------
ISO/TS 16774-2:2016(E)

Introduction
This Technical Specification is linked to ISO/TR 16475. ISO/TR 16475 outlines 6 basic properties
and the required performance levels of water leakage repair materials, and ISO/TS 16774 proposes a
tentative, sample testing methods that are capable of evaluating the respective properties of the repair
materials.
The test methods in this Technical Specification are intended to serve as a reference for nations that
have not yet developed a test method on the 6 required performance properties of water leakage
repair materials. If other forms of test methods that are simpler, more accurate or more organized are
available, such methods are recommended for use instead. Many of the dependent variables outlined
in the reference test methods of this Technical Specification are subject to change in accordance to
the environmental conditions (temperature and humidity, chemical solution and concentration, width
of movement activity, water pressure or water flow velocity, etc.) outlined in the standards used in
respective countries.
For ISO/TS 16774-1, ISO/TS 16774-5 and ISO/TS 16774-6, for the purpose of objectively comparing the
performance of injected repair materials, artificial cracks of same width, height, and volume were used
to control the usage of repair materials for each testing cycle and enable repetition of the same test
methods under the same conditions.
© ISO 2016 – All rights reserved v

---------------------- Page: 5 ----------------------
TECHNICAL SPECIFICATION ISO/TS 16774-2:2016(E)
Test methods for repair materials for water-leakage cracks
in underground concrete structures —
Part 2:
Test method for chemical resistance
1 Scope
This part of ISO/TS 16774 specifies a laboratory test method for the qualitative determination of the
retention level of chemical resistance of repair materials in repaired cracks of concrete structures in
conditions where the material is either underwater or in contact with water that may have various
chemical components present.
2 Normative references
The following documents, in whole or in part, are normatively referenced in this document and are
indispensable for its application. For dated references, only the edition cited applies. For undated
references, the latest edition of the referenced document (including any amendments) applies.
ISO/TR 16475, Guidelines for the repair of water-leakage cracks in concrete structures
3 Terms and definitions
For the purposes of this document, the terms and definitions given in ISO/TR 16475 and the
following apply.
3.1
repair material for water-leakage cracks
grouting materials used to prevent water-leakages in concrete cracks
Note 1 to entry: In this Technical Specification, target ingredients are limited to injection materials outlined in
ISO/TR 16475.
4 Principle
A repair material’s resistance to chemical attacks is one of the fundamental properties that water-
leakage repair materials should possess. While repair materials can undergo chemical property
changes due to chemical attack, and moreover, harmful chemical substances can also corrode the repair
materials and reduce their repair performance in water-leakage cracks. This test method evaluates a
water-leakage repair material’s chemical resistance performance by determining if the tested material
can maintain as closely as possible its original mass after being exposed to various types of chemical
substances as a means to evaluate the material’s resistance against chemical corrosion. In this method,
comparing the mass difference of water leakage repair materials before and after chemical exposure
can be used to determine the repair material’s chemical resistance level. An example test method is
provided in Annex A.
The tested repair material sample prepared in a Petri dish is placed in a container and completely
immersed in chemical solutions for predetermined number of hours or days (values subject to change
in accordance to different national standards). The concentration of the tested chemical solution
follows the condition of the applied environment belonging to different national standards, meaning
test chemical substances that represent common chemical substances that are exposed to concrete
© ISO 2016 – All rights reserved 1

---------------------- Page: 6 ----------------------
ISO/TS 16774-2:2016(E)

material and repair materials, as well as exposure time and chemical concentration range values should
reflect the applicable environmental conditions.
Test specimens are treated so that they r
...

TECHNICAL ISO/TS
SPECIFICATION 16774-2
First edition
Test methods for repair materials for
water-leakage cracks in underground
concrete structures —
Part 2:
Test method for chemical resistance
Méthodes d’essai pour matériaux de réparation pour fissures dues à
l’eau dans les structures en béton souterraines —
Partie 2: Méthode d’essai de la résistance chimique
PROOF/ÉPREUVE
Reference number
ISO/TS 16774-2:2016(E)
©
ISO 2016

---------------------- Page: 1 ----------------------
ISO/TS 16774-2:2016(E)

COPYRIGHT PROTECTED DOCUMENT
© ISO 2016, Published in Switzerland
All rights reserved. Unless otherwise specified, no part of this publication may be reproduced or utilized otherwise in any form
or by any means, electronic or mechanical, including photocopying, or posting on the internet or an intranet, without prior
written permission. Permission can be requested from either ISO at the address below or ISO’s member body in the country of
the requester.
ISO copyright office
Ch. de Blandonnet 8 • CP 401
CH-1214 Vernier, Geneva, Switzerland
Tel. +41 22 749 01 11
Fax +41 22 749 09 47
copyright@iso.org
www.iso.org
ii © ISO 2016 – All rights reserved

---------------------- Page: 2 ----------------------
ISO/TS 16774-2:2016(E)

Contents Page
Foreword .iv
Introduction .v
1 Scope . 1
2 Normative references . 1
3 Terms and definitions . 1
4 Principle . 1
5 Apparatus . 2
6 Preparation . 2
6.1 Test specimens . 2
6.2 Chemical substance . 2
6.3 Ambient conditions . 2
7 Procedure. 3
8 Expression of results . 3
9 Test report . 3
9.1 Information on the repair material of the test target . 3
9.1.1 General. 3
9.1.2 Other information . 4
9.2 Information on the test . 4
Annex A (informative) Example test method . 5
Bibliography . 8
© ISO 2016 – All rights reserved PROOF/ÉPREUVE iii

---------------------- Page: 3 ----------------------
ISO/TS 16774-2:2016(E)

Foreword
ISO (the International Organization for Standardization) is a worldwide federation of national standards
bodies (ISO member bodies). The work of preparing International Standards is normally carried out
through ISO technical committees. Each member body interested in a subject for which a technical
committee has been established has the right to be represented on that committee. International
organizations, governmental and non-governmental, in liaison with ISO, also take part in the work.
ISO collaborates closely with the International Electrotechnical Commission (IEC) on all matters of
electrotechnical standardization.
The procedures used to develop this document and those intended for its further maintenance are
described in the ISO/IEC Directives, Part 1. In particular the different approval criteria needed for the
different types of ISO documents should be noted. This document was drafted in accordance with the
editorial rules of the ISO/IEC Directives, Part 2 (see www.iso.org/directives).
Attention is drawn to the possibility that some of the elements of this document may be the subject of
patent rights. ISO shall not be held responsible for identifying any or all such patent rights. Details of
any patent rights identified during the development of the document will be in the Introduction and/or
on the ISO list of patent declarations received (see www.iso.org/patents).
Any trade name used in this document is information given for the convenience of users and does not
constitute an endorsement.
For an explanation on the meaning of ISO specific terms and expressions related to conformity assessment,
as well as information about ISO’s adherence to the World Trade Organization (WTO) principles in the
Technical Barriers to Trade (TBT) see the following URL: www.iso.org/iso/foreword.html.
The committee responsible for this document is ISO/TC 71, Concrete, reinforced concrete and pre-
stressed concrete, Subcommittee SC 7, Maintenance and repair of concrete structures.
ISO/TS 16774 consist of the following parts, under the general title Test methods for repair materials for
water-leakage cracks in underground concrete structures:
— Part 2: Test method for chemical resistance
— Part 3: Test method for water (wash out) resistance
— Part 4: Test method for adhesion on wet concrete surface
The following parts are under preparation:
— Part 1: Test method for thermal stability
— Part 5: Test method for watertightness
— Part 6: Test method for response to the substrate movement
iv PROOF/ÉPREUVE © ISO 2016 – All rights reserved

---------------------- Page: 4 ----------------------
ISO/TS 16774-2:2016(E)

Introduction
This Technical Specification is linked to ISO/TR 16475. ISO/TR 16475 outlines 6 basic properties
and the required performance levels of water leakage repair materials, and ISO/TS 16774 proposes a
tentative, sample testing methods that are capable of evaluating the respective properties of the repair
materials.
The test methods in this Technical Specification are intended to serve as a reference for nations that
have not yet developed a test method on the 6 required performance properties of water leakage
repair materials. If other forms of test methods that are simpler, more accurate or more organized are
available, such methods are recommended for use instead. Many of the dependent variables outlined
in the reference test methods of this Technical Specification are subject to change in accordance to
the environmental conditions (temperature and humidity, chemical solution and concentration, width
of movement activity, water pressure or water flow velocity, etc.) outlined in the standards used in
respective countries.
For ISO/TS 16774-1, ISO/TS 16774-5 and ISO/TS 16774-6, for the purpose of objectively comparing the
performance of injected repair materials, artificial cracks of same width, height, and volume were used
to control the usage of repair materials for each testing cycle and enable repetition of the same test
methods under the same conditions.
© ISO 2016 – All rights reserved PROOF/ÉPREUVE v

---------------------- Page: 5 ----------------------
TECHNICAL SPECIFICATION ISO/TS 16774-2:2016(E)
Test methods for repair materials for water-leakage cracks
in underground concrete structures —
Part 2:
Test method for chemical resistance
1 Scope
This part of ISO/TS 16774 specifies a laboratory test method for the qualitative determination of the
retention level of chemical resistance of repair materials in repaired cracks in conditions where the
material is either underwater or in contact with water that may have various chemical components
present.
2 Normative references
The following documents, in whole or in part, are normatively referenced in this document and are
indispensable for its application. For dated references, only the edition cited applies. For undated
references, the latest edition of the referenced document (including any amendments) applies.
ISO/TR 16475, Guidelines for the repair of water-leakage cracks in concrete structures
3 Terms and definitions
For the purposes of this document, the terms and definitions given in ISO/TR 16475 and the
following apply.
3.1
repair material for water-leakage cracks
grouting materials used to prevent water-leakages in concrete cracks
Note 1 to entry: In this Technical Specification, target ingredients are limited to injection materials outlined in
ISO/TR 16475.
4 Principle
A repair material’s resistance to chemical attacks is one of the fundamental properties that water-
leakage repair materials should possess. While repair materials can undergo chemical property changes
due to chemical attack, harmful chemical substances can also corrode the repair materials reducing
their repair performance in water-leakage cracks. This test method tests if a water-leakage repair
material can maintain as closely as possible its original mass after being exposed to various types of
chemical substances as a means to evaluate the material’s resistance against chemical corrosion. In this
method, comparing the mass difference of water leakage repair materials before and after chemical
exposure can be used to determine the repair material’s chemical resistance level. An example test
method is provided in Annex A.
The tested repair material sample prepared in a Petri dish is placed in a container and completely
immersed in chemical solutions for predetermined number of hours or days (values subject to change
in accordance to different national standards). The concentration of the tested chemical solution
follows the condition of the applied environment belonging to different national standards, meaning
test chemical substances that represent common chemical substances that are exposed to concrete
© ISO 2016 – All rights reserved PROOF/ÉPREUVE 1

---------------------- Page: 6 ----------------------
ISO/TS 16774-2:2016(E)

material and repair materials, as well as exposure time and chemical concentration range values should
reflect the actual environmental condition
...

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