Oilseed meals - Determination of oil content - Extraction method with hexane (or light petroleum) (ISO 734:2023)

ISO 734:2015 specifies a method for the determination of the hexane extract (or light-petroleum extract), called "oil content", of meals (excluding compounded products) obtained by the extraction of oil from oilseeds by pressure or solvents.

Ölsamenschrote - Bestimmung des Ölgehaltes - Extraktionsverfahren mit Hexan (oder Petrolether) (ISO 734:2023)

Dieses Dokument legt ein Verfahren zur Bestimmung des Hexanextrakts (oder des Petroletherextrakts), genannt „Ölgehalt“, von Extraktionsschroten (ausgeschlossen sind Mischprodukte) fest, die bei der Ölgewinnung durch Pressen oder bei Lösemittelextraktionen aus Ölsamen anfallen.

Tourteaux de graines oléagineuses - Détermination de la teneur en huile - Méthode par extraction à l'hexane (ou à l'éther de pétrole) (ISO 734:2023)

ISO 734:2015 spécifie une méthode de détermination de l'extrait à l'hexane (ou à l'éther de pétrole), dite «teneur en huile» des tourteaux (à l'exclusion des produits composés) provenant de l'extraction de l'huile des graines oléagineuses par pression ou solvant.

Obroki iz semen oljnic - Določevanje vsebnosti olja - Metoda ekstrakcije s heksanom (ali petroletrom) (ISO 734:2023)

Standard ISO 734:2015 opredeljuje metodo za ugotavljanje ekstrakta heksana (ali petroletra), imenovano »vsebnost olja«, v ostankih (vključno z mešanimi izdelki), pridobljenih z ekstrakcijo olja iz semen oljnic pod tlakom ali s pomočjo topil.

General Information

Status
Published
Public Enquiry End Date
30-May-2022
Publication Date
05-Apr-2023
Current Stage
6060 - National Implementation/Publication (Adopted Project)
Start Date
29-Mar-2023
Due Date
03-Jun-2023
Completion Date
06-Apr-2023

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SLOVENSKI STANDARD
SIST EN ISO 734:2023
01-maj-2023
Obroki iz semen oljnic - Določevanje vsebnosti olja - Metoda ekstrakcije s
heksanom (ali petroletrom) (ISO 734:2023)
Oilseed meals - Determination of oil content - Extraction method with hexane (or light
petroleum) (ISO 734:2023)
Ölsamenschrote - Bestimmung des Ölgehaltes - Extraktionsverfahren mit Hexan (oder
Petrolether) (ISO 734:2023)
Tourteaux de graines oléagineuses - Détermination de la teneur en huile - Méthode par
extraction à l'hexane (ou à l'éther de pétrole) (ISO 734:2023)
Ta slovenski standard je istoveten z: EN ISO 734:2023
ICS:
67.200.20 Oljnice Oilseeds
SIST EN ISO 734:2023 en,fr,de
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.

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SIST EN ISO 734:2023

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SIST EN ISO 734:2023


EN ISO 734
EUROPEAN STANDARD

NORME EUROPÉENNE

February 2023
EUROPÄISCHE NORM
ICS 67.200.20 Supersedes EN ISO 734:2015
English Version

Oilseed meals - Determination of oil content - Extraction
method with hexane (or light petroleum) (ISO 734:2023)
Tourteaux de graines oléagineuses - Détermination de Ölsamenschrote - Bestimmung des Ölgehaltes -
la teneur en huile - Méthode par extraction à l'hexane Extraktionsverfahren mit Hexan (oder Petrolether)
(ou à l'éther de pétrole) (ISO 734:2023) (ISO 734:2023)
This European Standard was approved by CEN on 13 February 2023.

CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this
European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references
concerning such national standards may be obtained on application to the CEN-CENELEC Management Centre or to any CEN
member.

This European Standard exists in three official versions (English, French, German). A version in any other language made by
translation under the responsibility of a CEN member into its own language and notified to the CEN-CENELEC Management
Centre has the same status as the official versions.

CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia,
Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway,
Poland, Portugal, Republic of North Macedonia, Romania, Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland, Türkiye and
United Kingdom.





EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION

EUROPÄISCHES KOMITEE FÜR NORMUNG

CEN-CENELEC Management Centre: Rue de la Science 23, B-1040 Brussels
© 2023 CEN All rights of exploitation in any form and by any means reserved Ref. No. EN ISO 734:2023 E
worldwide for CEN national Members.

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SIST EN ISO 734:2023
EN ISO 734:2023 (E)
Contents Page
European foreword . 3

2

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SIST EN ISO 734:2023
EN ISO 734:2023 (E)
European foreword
This document (EN ISO 734:2023) has been prepared by Technical Committee ISO/TC 34 "Food
products" in collaboration with Technical Committee CEN/TC 307 “Oilseeds, vegetable and animal fats
and oils and their by-products - Methods of sampling and analysis” the secretariat of which is held by
AFNOR.
This European Standard shall be given the status of a national standard, either by publication of an
identical text or by endorsement, at the latest by August 2023, and conflicting national standards shall
be withdrawn at the latest by August 2023.
Attention is drawn to the possibility that some of the elements of this document may be the subject of
patent rights. CEN shall not be held responsible for identifying any or all such patent rights.
This document supersedes EN ISO 734:2015.
Any feedback and questions on this document should be directed to the users’ national standards
body/national committee. A complete listing of these bodies can be found on the CEN website.
According to the CEN-CENELEC Internal Regulations, the national standards organizations of the
following countries are bound to implement this European Standard: Austria, Belgium, Bulgaria,
Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland,
Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Republic of
North Macedonia, Romania, Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland, Türkiye and the
United Kingdom.
Endorsement notice
The text of ISO 734:2023 has been approved by CEN as EN ISO 734:2023 without any modification.


3

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SIST EN ISO 734:2023

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SIST EN ISO 734:2023
INTERNATIONAL ISO
STANDARD 734
Third edition
2023-01
Oilseed meals — Determination of oil
content — Extraction method with
hexane (or light petroleum)
Tourteaux de graines oléagineuses — Détermination de la teneur en
huile — Méthode par extraction à l'hexane (ou à l'éther de pétrole)
Reference number
ISO 734:2023(E)
© ISO 2023

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SIST EN ISO 734:2023
ISO 734:2023(E)
COPYRIGHT PROTECTED DOCUMENT
© ISO 2023
All rights reserved. Unless otherwise specified, or required in the context of its implementation, no part of this publication may
be reproduced or utilized otherwise in any form or by any means, electronic or mechanical, including photocopying, or posting on
the internet or an intranet, without prior written permission. Permission can be requested from either ISO at the address below
or ISO’s member body in the country of the requester.
ISO copyright office
CP 401 • Ch. de Blandonnet 8
CH-1214 Vernier, Geneva
Phone: +41 22 749 01 11
Email: copyright@iso.org
Website: www.iso.org
Published in Switzerland
ii
  © ISO 2023 – All rights reserved

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SIST EN ISO 734:2023
ISO 734:2023(E)
Contents Page
Foreword .iv
Introduction .v
1 Scope . 1
2 Normative references . 1
3 Terms and definitions . 1
4 Principle . 1
5 Reagents . 1
6 Apparatus . 2
7 Sampling . 2
8 Preparation of test sample . 3
9 Procedure .3
9.1 Number of determinations . 3
9.2 Test portion . 3
9.3 Pre-drying . 3
9.4 Determination . 3
9.4.1 Preparation of the flask . . . 3
9.4.2 First extraction . 3
9.4.3 Second extraction . 4
9.4.4 Elimination of solvent and weighing of the extract . 4
10 Expression of results . 4
11 Precision . 5
11.1 Interlaboratory test . . 5
11.2 Repeatability . 5
11.3 Reproducibility . 5
12 Test report . 5
Annex A (informative) Results of an interlaboratory test . 7
Bibliography . 8
iii
© ISO 2023 – All rights reserved

---------------------- Page: 9 ----------------------
SIST EN ISO 734:2023
ISO 734:2023(E)
Foreword
ISO (the International Organization for Standardization) is a worldwide federation of national standards
bodies (ISO member bodies). The work of preparing International Standards is normally carried out
through ISO technical committees. Each member body interested in a subject for which a technical
committee has been established has the right to be represented on that committee. International
organizations, governmental and non-governmental, in liaison with ISO, also take part in the work.
ISO collaborates closely with the International Electrotechnical Commission (IEC) on all matters of
electrotechnical standardization.
The procedures used to develop this document and those intended for its further maintenance are
described in the ISO/IEC Directives, Part 1. In particular, the different approval criteria needed for the
different types of ISO documents should be noted. This document was drafted in accordance with the
editorial rules of the ISO/IEC Directives, Part 2 (see www.iso.org/directives).
Attention is drawn to the possibility that some of the elements of this document may be the subject of
patent rights. ISO shall not be held responsible for identifying any or all such patent rights. Details of
any patent rights identified during the development of the document will be in the Introduction and/or
on the ISO list of patent declarations received (see www.iso.org/patents).
Any trade name used in this document is information given for the convenience of users and does not
constitute an endorsement.
For an explanation of the voluntary nature of standards, the meaning of ISO specific terms and
expressions related to conformity assessment, as well as information about ISO’s adherence to
the World Trade Organization (WTO) principles in the Technical Barriers to Trade (TBT), see
www.iso.org/iso/foreword.html.
This document was prepared by Technical Committee ISO/TC 34, Food products, Subcommittee
SC 2, Oleaginous seeds and fruits and oilseed meals, in collaboration with the European Committee for
Standardization (CEN) Technical Committee CEN/TC 307, Oilseeds, vegetable and animal fats and oils and
their by-products — Methods of sampling and analysis, in accordance with the Agreement on technical
cooperation between ISO and CEN (Vienna Agreement).
This third edition cancels and replaces the second edition (ISO 734:2015), which has been technically
revised in order to include some safety warnings.
Any feedback or questions on this document should be directed to the user’s national standards body. A
complete listing of these bodies can be found at www.iso.org/members.html.
iv
  © ISO 2023 – All rights reserved

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SIST EN ISO 734:2023
ISO 734:2023(E)
Introduction
A method for the determination of the oil content of oilseeds is specified in ISO 659. To provide for the
control of oil production, this document specifies a reference method f
...

SLOVENSKI STANDARD
oSIST prEN ISO 734:2022
01-maj-2022
Obroki iz semen oljnic - Določevanje vsebnosti olja - Metoda ekstrakcije s
heksanom (ali petroletrom) (ISO/DIS 734:2022)
Oilseed meals - Determination of oil content - Extraction method with hexane (or light
petroleum) (ISO/DIS 734:2022)
Ölsamenschrote - Bestimmung des Ölgehaltes - Extraktionsverfahren mit Hexan (oder
Petrolether) (ISO/DIS 734:2022)
Tourteaux de graines oléagineuses - Détermination de la teneur en huile - Méthode par
extraction à l'hexane (ou à l'éther de pétrole) (ISO/DIS 734:2022)
Ta slovenski standard je istoveten z: prEN ISO 734
ICS:
67.200.20 Oljnice Oilseeds
oSIST prEN ISO 734:2022 en,fr,de
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.

---------------------- Page: 1 ----------------------
oSIST prEN ISO 734:2022

---------------------- Page: 2 ----------------------
oSIST prEN ISO 734:2022
DRAFT INTERNATIONAL STANDARD
ISO/DIS 734
ISO/TC 34/SC 2 Secretariat: AFNOR
Voting begins on: Voting terminates on:
2022-03-16 2022-06-08
Oilseed meals — Determination of oil content — Extraction
method with hexane (or light petroleum)
Tourteaux de graines oléagineuses — Détermination de la teneur en huile — Méthode par extraction à
l'hexane (ou à l'éther de pétrole)
ICS: 67.200.20
This document is circulated as received from the committee secretariat.
THIS DOCUMENT IS A DRAFT CIRCULATED
FOR COMMENT AND APPROVAL. IT IS
ISO/CEN PARALLEL PROCESSING
THEREFORE SUBJECT TO CHANGE AND MAY
NOT BE REFERRED TO AS AN INTERNATIONAL
STANDARD UNTIL PUBLISHED AS SUCH.
IN ADDITION TO THEIR EVALUATION AS
BEING ACCEPTABLE FOR INDUSTRIAL,
TECHNOLOGICAL, COMMERCIAL AND
USER PURPOSES, DRAFT INTERNATIONAL
STANDARDS MAY ON OCCASION HAVE TO
BE CONSIDERED IN THE LIGHT OF THEIR
POTENTIAL TO BECOME STANDARDS TO
WHICH REFERENCE MAY BE MADE IN
Reference number
NATIONAL REGULATIONS.
ISO/DIS 734:2022(E)
RECIPIENTS OF THIS DRAFT ARE INVITED
TO SUBMIT, WITH THEIR COMMENTS,
NOTIFICATION OF ANY RELEVANT PATENT
RIGHTS OF WHICH THEY ARE AWARE AND TO
PROVIDE SUPPORTING DOCUMENTATION. © ISO 2022

---------------------- Page: 3 ----------------------
oSIST prEN ISO 734:2022
ISO/DIS 734:2022(E)
COPYRIGHT PROTECTED DOCUMENT
© ISO 2022
All rights reserved. Unless otherwise specified, or required in the context of its implementation, no part of this publication may
be reproduced or utilized otherwise in any form or by any means, electronic or mechanical, including photocopying, or posting on
the internet or an intranet, without prior written permission. Permission can be requested from either ISO at the address below
or ISO’s member body in the country of the requester.
ISO copyright office
CP 401 • Ch. de Blandonnet 8
CH-1214 Vernier, Geneva
Phone: +41 22 749 01 11
Email: copyright@iso.org
Website: www.iso.org
Published in Switzerland
ii
  © ISO 2022 – All rights reserved

---------------------- Page: 4 ----------------------
oSIST prEN ISO 734:2022
ISO/DIS 734:2022(E)
Contents Page
Foreword .iv
Introduction .v
1 Scope . 1
2 Normative references . 1
3 Terms and definitions . 1
4 Principle . 1
5 Reagents . 1
6 Apparatus . 1
7 Sampling . 2
8 Preparation of test sample . 2
9 Procedure .3
9.1 Number of determinations . 3
9.2 Test portion . 3
9.3 Pre-drying . 3
9.4 Determination . 3
9.4.1 Preparation of the flask . . . 3
9.4.2 First extraction . 3
9.4.3 Second extraction . 3
9.4.4 Elimination of solvent and weighing of the extract . 4
10 Expression of results . 4
11 Precision . 5
11.1 Interlaboratory test . . 5
11.2 Repeatability . 5
11.3 Reproducibility . 5
12 Test report . 5
Annex A (informative) Results of an interlaboratory test . 6
Bibliography . 7
iii
© ISO 2022 – All rights reserved

---------------------- Page: 5 ----------------------
oSIST prEN ISO 734:2022
ISO/DIS 734:2022(E)
Foreword
ISO (the International Organization for Standardization) is a worldwide federation of national standards
bodies (ISO member bodies). The work of preparing International Standards is normally carried out
through ISO technical committees. Each member body interested in a subject for which a technical
committee has been established has the right to be represented on that committee. International
organizations, governmental and non-governmental, in liaison with ISO, also take part in the work.
ISO collaborates closely with the International Electrotechnical Commission (IEC) on all matters of
electrotechnical standardization.
The procedures used to develop this document and those intended for its further maintenance are
described in the ISO/IEC Directives, Part 1. In particular the different approval criteria needed for the
different types of ISO documents should be noted. This document was drafted in accordance with the
editorial rules of the ISO/IEC Directives, Part 2 (see www.iso.org/directives).
Attention is drawn to the possibility that some of the elements of this document may be the subject of
patent rights. ISO shall not be held responsible for identifying any or all such patent rights. Details of
any patent rights identified during the development of the document will be in the Introduction and/or
on the ISO list of patent declarations received (see www.iso.org/patents).
Any trade name used in this document is information given for the convenience of users and does not
constitute an endorsement.
For an explanation on the meaning of ISO specific terms and expressions related to conformity
assessment, as well as information about ISO's adherence to the WTO principles in the Technical
Barriers to Trade (TBT) see the following URL: Foreword - Supplementary information
The committee responsible for this document is ISO/TC 34, Food products, Subcommittee SC 2,
Oleaginous seeds and fruits and oilseed meals.
This third edition cancels and replaces ISO 734:2015, which has been revised in order to include some
safety warnings.
iv
  © ISO 2022 – All rights reserved

---------------------- Page: 6 ----------------------
oSIST prEN ISO 734:2022
ISO/DIS 734:2022(E)
Introduction
A method for the determination of the oil content of oilseeds has been specified in ISO 659. It is
therefore necessary to provide for control of oil production by establishing a reference method for the
determination of the oil content of oilseed meals in the same way.
v
© ISO 2022 – All rights reserved

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oSIST prEN ISO 734:2022

---------------------- Page: 8 ----------------------
oSIST prEN ISO 734:2022
DRAFT INTERNATIONAL STANDARD ISO/DIS 734:2022(E)
Oilseed meals — Determination of oil content — Extraction
method with hexane (or light petroleum)
1 Scope
This International Standard specifies a method for the determination of the hexane extract (or light-
petroleum extract), called “oil content”, of meals (excluding compounded products) obtained by the
extraction of oil from oilseeds by pressure or solvents.
2 Normative references
The following documents, in whole or in part, are normatively referenced in this document and are
indispensable for its application. For dated references, only the edition cited applies. For undated
references, the latest edition of the referenced document (including any amendments) applies.
ISO 771, Oilseed meals — Determination of moisture and volatile matter content
ISO 5502, Oilseed residues — Preparation of test samples
3 Terms and definitions
For the purposes of this document, the following terms and definitions apply.
3.1
oil content
all of the substances extracted under the operating conditions specified in this International Standard,
and expressed as a mass fraction, in percent, of the product as received
Note 1 to entry: The oil content may also be expressed relative to dry matter.
4 Principle
A test portion of the product is extracted in a suitable apparatus, with technical hexane o
...

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