CEN/TS 17083:2017

Foodstuffs - Determination of acrylamide in food and coffee by gas chromatography-mass spectrometry (GC-MS)

This Technical Specification specifies a method for the determination of acrylamide in cereal-based products, potato-based products and coffee by gas-chromatography mass spectrometry (GC-MS).
The method has been single-laboratory validated via the analysis of spiked samples (French fries (uncooked), bread, water biscuit, infant cereal, biscuit, green coffee, roast coffee and instant coffee), ranging from 30 μg/kg to 1 500 μg/kg acrylamide.
The results from the single laboratory validation were obtained by a laboratory with significant experience in acrylamide analysis. In addition, this method has also been studied by inter laboratory trial via the analysis of samples containing incurred acrylamide, ranging from approximately 200 μg/kg to 2 000 μg/kg. Critical points of the method are identified in 7.5 and Clause 8.

Lebensmittel - Bestimmung von Acrylamid in Lebensmitteln und Kaffee mit Gaschromatographie-Massenspektrometrie (GC-MS)

Diese Technische Spezifikation legt ein Verfahren zur Bestimmung von Acrylamid in Getreideerzeugnissen, Kartoffelerzeugnissen und Kaffee durch Gaschromatographie gekoppelt mit Massen¬spektrometrie (GC MS) fest.
Dieses Verfahren wurde in einer Einzellaborvalidierung durch die Analyse von aufgestockten Proben (Pommes frites (ungegart), Brot, Kräcker, Getreidebeikost, Kekse, Rohkaffee, Röstkaffee und löslicher Kaffee) im Bereich von 30 μg/kg bis 1 500 μg/kg Acrylamid untersucht.
Die Ergebnisse der Einzellaborvalidierung wurden von einem Labor mit umfangreicher Erfahrung in der Acrylamid Analytik erzielt. Außerdem wurde dieses Verfahren auch in einem Ringversuch durch Untersuchung von Proben mit einem Anteil an entstandenem Acrylamid von etwa 200 μg/kg bis 2 000 μg/kg untersucht. Kritische Punkte des Verfahrens werden in 7.5 und Abschnitt 8 benannt.

Produits alimentaires - Dosage par CG-SM des produits alimentaires et café avec GC-MS

Živila - Določevanje akrilamida v živilih in kavi s plinsko kromatografijo/masno spektrometrijo (GC-MS)

Ta tehnična specifikacija opredeljuje metodo za določanje akrilamida v žitnih proizvodih, izdelkih iz krompirja in kavi s plinsko kromatografijo/masno spektrometrijo (GC-MS).
Metoda je bila validirana v laboratoriju z analizo primešanih vzorcev (krompirček, (nekuhan), kruh, krekerji, žita za dojenčke, piškoti, surova kava, pražena in instant kava) v razponu 30–1500 μg/kg akrilamida.
Rezultati validacije laboratorija so bili pridobljeni v laboratoriju z bogatimi izkušnjami z analizo akrilamida. Poleg tega je bila ta metoda raziskana tudi z medlaboratorijskim preskusom z analizo vzorcev, ki so vsebovali akrilamid v razponu približno 200–2000 μg/kg. Kritične točke metode so navedene v točkah 7.5 in 8.

General Information

• Status: Published
• Publication Date: 06-Jun-2017
• ICS: 67.050 - General methods of tests and analysis for food products
• ICS: 67.060 - Cereals, pulses and derived products
• ICS: 67.080.20 - Vegetables and derived products
• ICS: 67.140.20 - Coffee and coffee substitutes
• Technical Committee: CEN/TC 275 - Food analysis - Horizontal methods
• Drafting Committee: CEN/TC 275/WG 13 - Neoformed contaminants
• Current Stage: 9020 - Submission to 2 Year Review Enquiry - Review Enquiry
• Start Date: 15-Apr-2024
• Completion Date: 15-Apr-2024
• Directive: 882/2004 - Regulation (EC) No 882/2004 of the European Parliament and of the Council of 29 April 2004 onofficial controls performed to ensure the verification of compliance with feed and food law, animal health and animal welfare rules
• Mandate: M/463 - Mandate for Standardisation addressed to CEN for the methods of analysis for food contaminants
• Ref Project: SIST-TS CEN/TS 17083:2017 - Foodstuffs - Determination of acrylamide in food and coffee by gas chromatography-mass spectrometry (GC-MS)

Standards Content (Sample)

SLOVENSKI STANDARD
SIST-TS CEN/TS 17083:2017
01-september-2017
äLYLOD'RORþHYDQMHDNULODPLGDYåLYLOLKLQNDYLVSOLQVNRNURPDWRJUDILMRPDVQR
VSHNWURPHWULMR*&06
Foodstuffs - Determination of acrylamide in food and coffee by gas chromatography-
mass spectrometry (GC-MS)
Lebensmittel - Bestimmung von Acrylamid in Lebensmitteln und Kaffee mit
Gaschromatographie-Massenspektrometrie (GC-MS)
Produits alimentaires - Dosage par CG-SM des produits alimentaires et café avec GC-
MS
Ta slovenski standard je istoveten z: CEN/TS 17083:2017
ICS:
67.050 Splošne preskusne in General methods of tests and
analizne metode za živilske analysis for food products
proizvode
71.040.50 Fizikalnokemijske analitske Physicochemical methods of
metode analysis
SIST-TS CEN/TS 17083:2017 en,fr,de
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.

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SIST-TS CEN/TS 17083:2017

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SIST-TS CEN/TS 17083:2017


CEN/TS 17083
TECHNICAL SPECIFICATION

SPÉCIFICATION TECHNIQUE

June 2017
TECHNISCHE SPEZIFIKATION
ICS 67.050; 67.060; 67.140.20; 67.080.20
English Version

Foodstuffs - Determination of acrylamide in food and
coffee by gas chromatography-mass spectrometry (GC-MS)
Produits alimentaires - Dosage par CG-SM des produits Lebensmittel - Bestimmung von Acrylamid in
alimentaires et café avec GC-MS Lebensmitteln und Kaffee mit Gaschromatographie-
Massenspektrometrie (GC-MS)
This Technical Specification (CEN/TS) was approved by CEN on 14 May 2017 for provisional application.

The period of validity of this CEN/TS is limited initially to three years. After two years the members of CEN will be requested to
submit their comments, particularly on the question whether the CEN/TS can be converted into a European Standard.

CEN members are required to announce the existence of this CEN/TS in the same way as for an EN and to make the CEN/TS
available promptly at national level in an appropriate form. It is permissible to keep conflicting national standards in force (in
parallel to the CEN/TS) until the final decision about the possible conversion of the CEN/TS into an EN is reached.

CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia,
Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania,
Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland,
Turkey and United Kingdom.





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© 2017 CEN All rights of exploitation in any form and by any means reserved Ref. No. CEN/TS 17083:2017 E
worldwide for CEN national Members.

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SIST-TS CEN/TS 17083:2017
CEN/TS 17083:2017 (E)
Contents Page
European foreword . 3
1 Scope . 4
2 Normative references . 4
3 Principle . 4
4 Reagents . 4
5 Standard solution preparation . 6
6 Apparatus . 7
7 Procedure. 8
8 GC-MS analysis . 10
9 Calculating and reporting . 12
10 Test report . 12
11 Precision data .
...